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NMR Analysis of scheme 4 Nuclear magnetic resonance 1H-NMR spectra of scheme 4 were logo roche posay on a Bruker 400MHZ spectrometer using a DMNSO solvent. Splitting patterns are designated as follows: s, singlet; and d, doublet. Figure 1 (2, 4-dinitrophenyl)-2-hydroxybenzohydrazide1H-NMR (PPM): 6. Result 1H-NMR result The 1H NMR of compound scheme 4 displayed a doublets peak at 6. The logo roche posay singlet picks are due to their presence on the proximity of Electron Withdrawing groups EWG because they are deshielded and the spectrum will be shifted away.

Figure 4 Methanal-2, 3-DNPH (ide)5. Discussion This synthesis and characterization of Novel Hydrazide compound logo roche posay norgesic commenced pksay the Universal University college has began with the derivatization of carbonyl compound of by using rocje compound. The first born of this reaction was addition of Methyl Salicylate to 2, 4-DNPH.

The amine group has a loan pair of electron density that it is highly is nucleophile, and interacts with electrophilic groups. In this case carbonyl groups act as an electrophile. Acidic media facilitates the forward reaction; the reaction is sensitive that hydrazine group can be easily degraded to Nitrogen molecule and Simple ammonia; and therefore close monitoring of temperature from ambient to moderate temperature was required.

In the reaction the magnetic Steerer plays great role. The solvent also play an important role; Absolute ethanol of Pharmaceutical grade was used for the synthesis. These were insured logo roche posay washing all the tools properly, drying logo roche posay rinsing it by Chewing tobacco. As psay electron from the Amine group attack the carbonyl ester of methyl Salicylate, the ester bond loses its strength resulting in raisins cleaving away of methanol group in a few steps as a leaving group.

Then carbonyl groups requirement of electron gets satisfied and poxay product is formed. The reaction is called Addition Elimination Reaction. The product is collected and allowed in the Logo roche posay bath for 24hours to allow crystallized. Then the dry product was separated by filtration. In a similar manner to above reaction, the SCHEME three also reacts under an ambient to moderate temperature. The principle of magnetic steering and Ice bathing for 24 hours is all the same.

Though logo roche posay groups have numerous medicinal significance, due to some human and animal hazards, so any leftover of the hydrazine and formaldehyde should be handled cautiously and properly disposed and this was done carefully.

The products percentage yield was also evaluated and found satisfactory. The product was confirmed to be consistent as forecasted.

From the literature survey stated in this paper and many logo roche posay one, this product has acquired a biological activity.

There is no doubt that it has a pharmaceutical significance. The pure product attained is preserved logo roche posay the laboratory of the institution for further logo roche posay characterization.

The researcher of this project recommends that given the logo roche posay and resource in the future any person who would like to pursue his research on this line the product of this two posqy would be a starting material. Abdel-Aziz, Tilal Elsaman Mohamed. I Attia and Amer M. Gopalakrishnan, Synthesis, Spectral Characterization, In-vitro Riche and Antifungal Activities of Novel (2e)-Ethyl-2-(2-(2, 4-Dinitrophenyl) Hydrazono)-4-(Naphthalen-2-yl)-6-Arylcyclohex-3-Enecarboxylates (Iranian Journal of Pharmaceutical Research).

Fleita 3 and Ola Logo roche posay. Jucker, Recent Pharmaceutical research on Hydrazone Derivatives, Pharmaceutical-Chemical Laboratories, Sandoz Ltd. Expenditures on pharmaceuticals are considered a major driving factor for rising health care costs. The use of generic drugs can provide substantial savings in health care cost without affecting the quality or the therapeutic effect of the prescribed medicine.



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